HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 69752797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 69750316 | HCID 69750316 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69752797 | HCID 69752797 | 100% |
Reaction Steps
8-(2-(2,6-dimethylphenyl)ethenyl)-2,3-dimethylimidazo[1,2-a]pyridine was solved in methanol (3 ml) and ethanol (2 ml) and Pd/C (10%) (40 mg) was added. The mixture was hydrogenated at room temperature and atmospheric pressure until the uptake of hydrogen ceased. Following filtration through celite, the solvents were evaporated under reduced pressure to give the title compound, (0.069 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06579884B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-a51584eaff8143cb98b9bd83724d369d |
| Source note | uspto-grants-2003_06 |