HCID 22312692, compound → HCID 86584980, compound

Participants

Reaction Steps

Following General Procedure I above using cyclopentyl-α-hydroxyacetic acid (Example P) and 3-(L-alaninyl)-amino-2,4-dioxo-1,5-bis-phenyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine hydrochloride (Example 8-W), the tide compound was prepared as a white solid (melting point=139-149° C.). Purification was by flash chromatography eluting with CH2Cl2/EtOAc (1:2). Rf=0.50 and 0.39 (CH2Cl2/EtOAc, 1:2).

Provenance & Evidence