Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Allylamine | HCID 7853 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23085564 | HCID 23085564 | — |
Reaction Steps
A four-necked separable flask with a stirrer, a thermometer and a Dimroth reflux cooling tube was charged with 252.8 g (2.5 mol) of a 97 wt % sulfuric acid aqueous solution and 46.2 g of water, and 142.8 g (2.5 mol) of a monoallylamine was dropwise added with stirring at 20 to 30° C. After the dropwise addition, the mixture was heated up to 45° C., to obtain a homogeneous monoallylamine sulfate solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06579933B1 |
|---|
| Source dataset | uspto-grants-2003_06 |
|---|
| ORD ID | ord-cfd1ab365c004def98ad43ba0ef9f9dd |
|---|
| Source note | uspto-grants-2003_06 |
|---|
