Sulfuric Acid → HCID 23085564, compound

HRID 1369903Notes

Reaction equation

HRID 1369903 reaction equation
[S:1](=[O:5])(=[O:4])([OH:3])[OH:2].[CH2:6]([NH2:9])[CH:7]=[CH2:8]>O>[S:1]([OH:5])([OH:4])(=[O:3])=[O:2].[CH2:6]([NH2:9])[CH:7]=[CH2:8]

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 7853Allylamine

Product 1

HCID 23085564HCID 23085564, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
25 °C

Procedure

A four-necked separable flask with a stirrer, a thermometer and a Dimroth reflux cooling tube was charged with 252.8 g (2.5 mol) of a 97 wt % sulfuric acid aqueous solution and 46.2 g of water, and 142.8 g (2.5 mol) of a monoallylamine was dropwise added with stirring at 20 to 30° C. After the dropwise addition, the mixture was heated up to 45° C., to obtain a homogeneous monoallylamine sulfate solution.

Workup

  1. temperatureA four-necked separable flask with a stirrer, a thermometer and a Dimroth reflux
  2. temperaturecooling tube
  3. additionwas dropwise added
  4. additionAfter the dropwise addition
  5. temperaturethe mixture was heated up to 45° C.

Sources & evidence

ORD record
ord-cfd1ab365c004def98ad43ba0ef9f9dd
Source dataset
uspto-grants-2003_06
Patent number
US06579933B1

Reaction notes

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