HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 86584687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86584687 | HCID 86584687 | — |
Reaction Steps
Under an argon atomosphere, 5 g of phenol was dissolved in 25 ml of hexane. This was added dropwise to 26.5 ml of a hexane solution containing 1.0 M trimethylaluminum at −20° C. over 1 hour. This was brought to room temperature and allowed to stand overnight. The precipitate was filtered and washed with hexane. Recrystallization from ether gave 4.36 g of methylaluminum diphenoxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06579956B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-44923f6f0eb740fa8e6647bda6349b63 |
| Source note | uspto-grants-2003_06 |