HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 18516903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 18516935 | HCID 18516935 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18516903 | HCID 18516903 | — |
Reaction Steps
4-[2-(1,2,3-Triazol-2-yl)ethoxy]aniline was prepared from 4-[2-(1,2,3-triazol-2-yl)ethoxy]nitrobenzene (10.5 g, 44.8 mmol) and 10% palladium on charcoal (1.5 g) in a manner similar to the aniline intermediate of Example 12 to give the desired material (4.91 g) as a yellow solid m.p. 159°. δH (CDCl3) 7.62 (2H, s), 6.73-6.58 (4H, m), 4.77 (2H, t, J 5.8 Hz), 4.40 (2H, t, J 5.8 Hz) 3.43 (2H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06579983B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-5a3ca6a9f1fd4b72b51d9751b2d48ccb |
| Source note | uspto-grants-2003_06 |