HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 9893962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 9893962 | HCID 9893962 | — |
| Product | HCID 9893962 | HCID 9893962 | 35% |
| Product | HCID 18511670 | HCID 18511670 | — |
Reaction Steps
The S-methylation of 1.5 g (3.5 mmol) of the preceding thiourea 9.2 with 240 μl of methyl iodide according to 1.2 results in the preparation of 690 mg (Yd: 35%) of the isothiourea of formula 9:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583159B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-eaeb1a7516a141b7aa0cc5a0f16ad5c0 |
| Source note | uspto-grants-2003_06 |