HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenyl isothiocyanate → HCID 18511660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenyl isothiocyanate | HCID 15241 | — |
| Reactant | HCID 11738079 | HCID 11738079 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18511660 | HCID 18511660 | — |
Reaction Steps
The condensation of 1.2 g (4 mmol) of 1-[4-(3,4-difluorophenoxy)butyl]-4-(methylamino)piperidine with 0.61 g (4 mmol) of 4-fluorophenyl isothiocyanate in THF according to the protocol of Example 1.1 gives 1.75 g (Yd: 95%) of a powder of formula 13.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583159B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-f8f04fa01aec4c30b0ccf2b80ad95483 |
| Source note | uspto-grants-2003_06 |