HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19107605, compound → HCID 18510821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19107605 | HCID 19107605 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18510821 | HCID 18510821 | 75.4% |
Reaction Steps
10% Pd-C (20 mg) was added to a solution of 3,3-bis(4-methoxyphenyl)-propenenitrile (50 mg), synthesized by the process described in a literature J. Med. Chem., 32, 1820 (1989), in dioxane (5 ml), followed by hydrogenation for 2 hr. Pd-C was removed by filtration through Celite. The solvent was then removed by distillation to give 3,3-bis(4-methoxyphenyl)-propanenitrile (38 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583144B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-eaa29f9fd39c4d1ea7598648279cd7ae |
| Source note | uspto-grants-2003_06 |