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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1370547Generated: October 30, 2026

HCID 19107605, compound → HCID 18510821, compound

https://huagongshe.com/reaction/1370547

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19107605HCID 19107605—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 18510821HCID 1851082175.4%

Reaction Steps

10% Pd-C (20 mg) was added to a solution of 3,3-bis(4-methoxyphenyl)-propenenitrile (50 mg), synthesized by the process described in a literature J. Med. Chem., 32, 1820 (1989), in dioxane (5 ml), followed by hydrogenation for 2 hr. Pd-C was removed by filtration through Celite. The solvent was then removed by distillation to give 3,3-bis(4-methoxyphenyl)-propanenitrile (38 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06583144B2
Source datasetuspto-grants-2003_06
ORD IDord-eaa29f9fd39c4d1ea7598648279cd7ae
Source noteuspto-grants-2003_06