HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Vinylpyridine → HCID 18511695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Vinylpyridine | HCID 7521 | — |
| Reactant | 3-Bromo-5-chloropyridin-2-amine | HCID 2763971 | — |
| Product | HCID 18511695 | HCID 18511695 | — |
Reaction Steps
The title compound was prepared from 3-bromo-5-chloro-2-pyridinamine and 2-vinylpyridine. Purification by column chromatography on silica gel eluting with methylene chloride—methanol (95:5) and repeated using hexane—EtOAc (70:30 to 50:50) as eluant gave a yellow solid:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583162B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-04df18f8f389442984e1312b3b75dfb4 |
| Source note | uspto-grants-2003_06 |