HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinylcyclohexane → HCID 18752902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinylcyclohexane | HCID 12757 | — |
| Reactant | 3-Bromo-5-chloropyridin-2-amine | HCID 2763971 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18752902 | HCID 18752902 | — |
Reaction Steps
The title compound was prepared from 3-bromo-5-chloro-2-pyridinamine and vinylcyclohexane. Purification by column chromatography on silica gel eluting with hexane—EtOAc (80:20) gave a pale yellow oil. An analytical sample was prepared by crystallisation from hexane:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583162B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-3342317b5d904046902f334d7245b3d8 |
| Source note | uspto-grants-2003_06 |