HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57310240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 86759031 | HCID 86759031 | — |
| Product | HCID 57310240 | HCID 57310240 | 32% |
Reaction Steps
The product from Example 9f (1.0 mmol, 450 mg) was dissolved in dioxane (5 mL). Six normal HCl (0.5 mL) was added, and the mixture was stirred one hour. Concentration followed by chromatography afforded the title compound as a glass (120 mg, 32%). MS MH+ calcd. for C17H18N2O6S 378, found 379.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583299B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-c0316885b1e04e1c8a135a92f05988b1 |
| Source note | uspto-grants-2003_06 |