HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131723933, compound → HCID 70016103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131723933 | HCID 131723933 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 70016103 | HCID 70016103 | 99.6% |
Reaction Steps
A solution of the title compound of Example 11a (17.9 g, 59.0 mmol) in glacial acetic acid (135 mL) and concentrated HCl (135 mL), was heated to 7 degrees C. for 2 hours. The solution was concentrated under a stream of N2 to yield the title compound as a white solid (17.0 g, quant. yield): MS MH+ calcd. for C11H12NO5SF: 290, found 290. HRMS calc. for C11H13NO5SF: 290.0499, found: 290.0520.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583299B1 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-f1589fde7d5e409b8cd06845c1ec40c0 |
| Source note | uspto-grants-2003_06 |