HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 2,4-DICHLOROBENZYL IODIDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 2,4-Dichlorobenzyl chloride | HCID 7212 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2,4-DICHLOROBENZYL IODIDE | HCID 518322 | — |
Reaction Steps
2,4-Dichloro-1-(chloromethyl)benzene (0.8 mmoles) in acetone (2 mL) was treated with NaI (0.48 g) and stirred at room temperature overnight. The solvent was removed under reduced pressure and the residue extracted with DMF to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583180B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-34b90f6442c24aa8a4a003c372b0e33b |
| Source note | uspto-grants-2003_06 |