Sodium Iodide → 2,4-DICHLOROBENZYL IODIDE

HRID 1370796Notes

Reaction equation

HRID 1370796 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9]Cl.[Na+].[I-:12]>CC(C)=O>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9][I:12]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 72122,4-Dichlorobenzyl chloride

Product 1

HCID 5183222,4-DICHLOROBENZYL IODIDE

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

2,4-Dichloro-1-(chloromethyl)benzene (0.8 mmoles) in acetone (2 mL) was treated with NaI (0.48 g) and stirred at room temperature overnight. The solvent was removed under reduced pressure and the residue extracted with DMF to provide the title compound.

Workup

  1. customThe solvent was removed under reduced pressure
  2. extractionthe residue extracted with DMF

Sources & evidence

ORD record
ord-34b90f6442c24aa8a4a003c372b0e33b
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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