HCID 18511975, compound → HCID 18512254, compound

Participants

Reaction Steps

The product from Example 6D and diisobutylaluminum hydride were processed as described in Example 38A to provide the title compound. 1H NMR (300 MHz, CDCl3) δ7.21 (m, 10H), 7.97 (t, J=8.0 Hz, 1H), 6.88 (dd, J=8.5, 1.0 Hz, 1H), 6.12 (s, 1H), 4.67 (d, J=8 Hz, 2H), 4.05 (s, 2H), 4.03 (s, 2H), 2. 96 (s, 3H), 2.37 (s, 2H; MS (APCI+) m/z 411 (M+H)+.

Provenance & Evidence