Ethyl Glycolate → HCID 86586232, compound

HRID 1370878Notes

Reaction equation

[F:1][C:2]1[CH:35]=[C:34]([F:36])[CH:33]=[CH:32][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:31]=[CH:30][C:20]([O:21][C:22]2[CH:23]=[C:24]([OH:29])[CH:25]=[C:26]([CH3:28])[CH:27]=2)=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15].[C:37]([O:41][CH2:42][CH3:43])(=[O:40])[CH2:38]O>>[F:1][C:2]1[CH:35]=[C:34]([F:36])[CH:33]=[CH:32][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:31]=[CH:30][C:20]([O:21][C:22]2[CH:23]=[C:24]([CH:25]=[C:26]([CH3:28])[CH:27]=2)[O:29][CH2:38][C:37]([O:41][CH2:42][CH3:43])=[O:40])=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15]

Participants

Reactant 2

HCID 12184Ethyl Glycolate

HCID 18512400HCID 18512400, compound

Product 1

HCID 86586232HCID 86586232, compound

Procedure

The product from Example 89E and ethyl glycolate were processed as described in Example 62A to provide the title compound.

Sources & evidence

ORD record: ord-d557764ab17b41d384beb37953f3b5b5
Source dataset: uspto-grants-2003_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06583180B2

Reaction notes

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