Ethyl Glycolate → HCID 86586233, compound

HRID 1370883Notes

Reaction equation

[F:1][C:2]1[CH:36]=[C:35]([F:37])[CH:34]=[CH:33][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:32]=[CH:31][C:20]([O:21][C:22]2[CH:23]=[C:24]([OH:30])[CH:25]=[C:26]([O:28][CH3:29])[CH:27]=2)=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15].[C:38]([O:42][CH2:43][CH3:44])(=[O:41])[CH2:39]O>>[F:1][C:2]1[CH:36]=[C:35]([F:37])[CH:34]=[CH:33][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:32]=[CH:31][C:20]([O:21][C:22]2[CH:23]=[C:24]([CH:25]=[C:26]([O:28][CH3:29])[CH:27]=2)[O:30][CH2:39][C:38]([O:42][CH2:43][CH3:44])=[O:41])=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15]

Participants

Reactant 2

HCID 12184Ethyl Glycolate

HCID 18512034HCID 18512034, compound

Product 1

HCID 86586233HCID 86586233, compound

Procedure

The product from Example 90E and ethyl glycolate were processed as described in Example 62A to provide the title compound. MS (ESI+) m/z 593 (M+H)+.

Sources & evidence

ORD record: ord-583df146c8f641db98240f63b1058170
Source dataset: uspto-grants-2003_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06583180B2

Reaction notes

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