Ethyl Glycolate → HCID 86586235, compound

HRID 1370891Notes

Reaction equation

HRID 1370891 reaction equation
[CH2:1]([N:8]([CH2:19][C:20]1[CH:33]=[CH:32][C:23]([O:24][C:25]2[CH:30]=[CH:29][C:28]([OH:31])=[CH:27][CH:26]=2)=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:34]([O:38][CH2:39][CH3:40])(=[O:37])[CH2:35]O>>[CH2:1]([N:8]([CH2:19][C:20]1[CH:33]=[CH:32][C:23]([O:24][C:25]2[CH:26]=[CH:27][C:28]([O:31][CH2:35][C:34]([O:38][CH2:39][CH3:40])=[O:37])=[CH:29][CH:30]=2)=[CH:22][CH:21]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([N+:15]([O-:17])=[O:16])[C:10]=1[CH3:18])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 12184Ethyl GlycolateHCID 18512025HCID 18512025, compound

Product 1

HCID 86586235HCID 86586235, compound

Procedure

The product from Example 60E and ethyl glycolate were processed as described in Example 62A to provide the title compound. MS (ESI+) m/z 527 (M+H)+.

Sources & evidence

ORD record
ord-11e1b79a8e4b4356b1f33772d82bac84
Source dataset
uspto-grants-2003_06
Patent number
US06583180B2

Reaction notes

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