6-Amino-1-hexanol → HCID 18512319, compound

Participants

Reaction Steps

The product from Example 104A and 6-amino-1-hexanol processed as described in Example 147 to provide the title compound. 1H NMR (500 MHz, DMSO-D) δ8.95 (s, 1 H), 7.73 (t, 1 H), 7.26 (m, 6 H), 7.19 (m, 3 H), 7.04 (t, 1 H), 6.96 (m, 2 H), 6.87 (m, 4 H), 4.03 (d, 4 H), 3.35 (m, 2 H), 3.00 (dd, 2 H), 2.91 (s, 3 H), 2.78 (t, 2 H), 2.39 (s, 3 H), 2.33 (t, 2 H), 1.37 (m, 4 H), 1.23 (m, 4 H); MS (APCI+) m/z 645 (M+H)+.

Provenance & Evidence