Ethyl Glycolate → HCID 86586237, compound

HRID 1370932Notes

Reaction equation

[F:1][C:2]1[CH:40]=[C:39]([F:41])[CH:38]=[CH:37][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:36]=[CH:35][C:20]([O:21][C:22]2[CH:23]=[CH:24][C:25]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[C:26]([OH:28])[CH:27]=2)=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15].[C:42]([O:46][CH2:47][CH3:48])(=[O:45])[CH2:43]O>>[F:1][C:2]1[CH:40]=[C:39]([F:41])[CH:38]=[CH:37][C:3]=1[CH2:4][N:5]([CH2:16][C:17]1[CH:36]=[CH:35][C:20]([O:21][C:22]2[CH:23]=[CH:24][C:25]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[C:26]([CH:27]=2)[O:28][CH2:43][C:42]([O:46][CH2:47][CH3:48])=[O:45])=[CH:19][CH:18]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:7]=1[CH3:15]

Participants

Reactant 2

HCID 12184Ethyl Glycolate

HCID 18512215HCID 18512215, compound

Product 1

HCID 86586237HCID 86586237, compound

Procedure

The product from Example 238F and ethyl glycolate were processed as described in Example 62A to provide the titled compound. MS (ESI+) m/z 597 (M+H)+.

Sources & evidence

ORD record: ord-ed9fbf8b5e3e48199b405e64a97f2d59
Source dataset: uspto-grants-2003_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06583180B2

Reaction notes

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