Ethyl Glycolate → HCID 86759034, compound

HRID 1370980Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([CH2:15][N:16]([CH2:27][C:28]3[CH:33]=[CH:32][C:31]([F:34])=[CH:30][C:29]=3[F:35])[C:17]3[CH:22]=[CH:21][CH:20]=[C:19]([N+:23]([O-:25])=[O:24])[C:18]=3[CH3:26])=[CH:11][CH:10]=2)=[CH:4][C:3]=1[OH:36].[C:37]([O:41][CH2:42][CH3:43])(=[O:40])[CH2:38]O>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([CH2:15][N:16]([CH2:27][C:28]3[CH:33]=[CH:32][C:31]([F:34])=[CH:30][C:29]=3[F:35])[C:17]3[CH:22]=[CH:21][CH:20]=[C:19]([N+:23]([O-:25])=[O:24])[C:18]=3[CH3:26])=[CH:11][CH:10]=2)=[CH:4][C:3]=1[O:36][CH2:38][C:37]([O:41][CH2:42][CH3:43])=[O:40]

Participants

Reactant 2

HCID 12184Ethyl Glycolate

HCID 18512336HCID 18512336, compound

Product 1

HCID 86759034HCID 86759034, compound

Procedure

The product from Example 323B and ethyl glycolate were processed as described in Example 62A to provide the title compound. MS (ESI+) m/z 641 (M+H)+.

Sources & evidence

ORD record: ord-95617e31525c4cde9638902b907ab6d1
Source dataset: uspto-grants-2003_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06583180B2

Reaction notes

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