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8-Hydroxyquinoline → Aluminium tri(quinolin-8-olate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 8-Hydroxyquinoline | HCID 1923 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Aluminum sulfate hexadecahydrate | HCID 23065692 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Aluminium tri(quinolin-8-olate) | HCID 90594 | 197.6% |
反応手順
To 93 g of water were added 25 g of aluminum sulfate hexadecahydrate and 35 g of 99% pure 8-hydroxyquinoline and the mixture was neutralized by dropwise addition of 29 g of a 33% solution of sodium hydroxide with stirring and allowed to react. The solid formed was collected by filtration, washed with water and dried to give 36 g of Alq3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06583583B1 |
| 出典データセット | uspto-grants-2003_06 |
| ORD ID | ord-b5b62ed6e0904eb8ba229573dda84fc8 |
| 出典メモ | uspto-grants-2003_06 |