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HRID1370984

反应详情

EQUATION

反应方程式

HRID 1370984 的结构方程式

REACTANTS

反应物

3
结构：Oc1cccc2cccnc12
HCID1923

8-Hydroxyquinoline

C9H7NO

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Al+3].[Al+3]
HCID23065692

未命名化合物

PRODUCTS

生成物

1
结构：[Al+3].[O-]c1cccc2cccnc12.[O-]c1cccc2cccnc12.[O-]c1cccc2cccnc12
HCID90594

Aluminium tris(quinolin-8-olate)

C27H18AlN3O3

收率 197.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

To 93 g of water were added 25 g of aluminum sulfate hexadecahydrate and 35 g of 99% pure 8-hydroxyquinoline and the mixture was neutralized by dropwise addition of 29 g of a 33% solution of sodium hydroxide with stirring and allowed to react. The solid formed was collected by filtration, washed with water and dried to give 36 g of Alq3.

WORKUP

后处理

  1. customto react
  2. customThe solid formed
  3. filtrationwas collected by filtration
  4. washwashed with water
  5. customdried