HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18510234, compound → HCID 18510257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18510234 | HCID 18510234 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18510257 | HCID 18510257 | — |
Reaction Steps
To a solution of isopropyl 4-[(E)-1-{4-[[di(tert-butoxy)phosphoryl](difluro)methyl]benzyl}-4-{4-[(diethoxyphosphoryl)(difluoro)methyl]phenyl}-1-(4-fluorobenzoyl)-3-butenyl]benzoate in ethyl acetate was added palladium on charcoal. The mixture ws then hydrogenated on a Parr apparatus at 50 psi. The reaction mixture was filtered and evaporated to give 0.02 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583126B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-9e3aff92614148df9c70b3378a7120d0 |
| Source note | uspto-grants-2003_06 |