HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 10305507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 88104241 | HCID 88104241 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 10305507 | HCID 10305507 | — |
Reaction Steps
The compound of Example 10 (0.080 g, 0.112 mmol) was treated with NaOH in THF/MeOH at 60° C. After a period of 18 h, Dowex H+ was added. After a few minutes, the resin was filtered and the solvent evaporated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06583126B2 |
| Source dataset | uspto-grants-2003_06 |
| ORD ID | ord-893e565d322648b48f0c99f827a98fa9 |
| Source note | uspto-grants-2003_06 |