HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 22479008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 4-(2-Hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butan-1-amine | HCID 22344437 | — |
| Product | HCID 22479008 | HCID 22479008 | 87.4% |
Reaction Steps
Using the general method of Example 146. Part B, 4-(2-hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butylamine (4.0 g, 12.3 mmol) was reacted with phenyl isocyanate (1.34 mL, 12.3 mmol) to provide 4.77 g of N-[4-(2-hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butyl]-N′-phenylurea.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157453B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-4f29333fc30d42dd8fa8cc8d60cce8ca |
| Source note | uspto-grants-2007_01 |