HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(Ethanesulfonyl)propan-1-amine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | tert-Butyl 3-(ethylsulfonyl)propylcarbamate | HCID 23089203 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 3-(Ethanesulfonyl)propan-1-amine hydrochloride | HCID 23089204 | — |
Reaction Steps
Intermediate 39 (0.275 g) was dissolved in 4M hydrogen chloride in dioxane (3 ml), and the solution was allowed to stand at 22° C. for 2 h. The solvent was evaporated in vacuo to give the title compound as a white solid (186 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-d288090551eb491dabb37bae96dc05ac |
| Source note | uspto-grants-2007_01 |