HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-isocyanatobenzoate → HCID 10138895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-isocyanatobenzoate | HCID 2733366 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | HCID 10138895 | HCID 10138895 | 90% |
Reaction Steps
Example 15 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and methyl 3-isocyanatobenzoate (0.0241 g) to give the title compound (0.037 g). LC-MS (System A): Rt 2.32 mins, Mass Spectrum m/z 452 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-c7da920a9c7943cbb4c170e761718f4d |
| Source note | uspto-grants-2007_01 |