HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylthio)phenyl isocyanate → N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}-N'-[3-(methylthio)phenyl]urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylthio)phenyl isocyanate | HCID 141418 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | N-{[4-(3,4-Dichlorobenzyl)morpholin-2-yl]methyl}-N'-[3-(methylthio)phenyl]urea | HCID 17984662 | — |
Reaction Steps
Example 18 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 1-isocyanato-3-(methylthio)benzene (18.8 μl) to give the title compound (0.0352 g). LC-MS (System A): Rt 2.41 mins, Mass Spectrum m/z 440 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-c093d6bbb31b49d5ac8cecd49646717b |
| Source note | uspto-grants-2007_01 |