HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenyl isocyanate → HCID 17984749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenyl isocyanate | HCID 75609 | — |
| Reactant | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Product | HCID 17984749 | HCID 17984749 | 76.8% |
Reaction Steps
Example 20 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 1-bromo-4-isocyanatobenzene (0.027 g) to give the title compound (0.033 g). LC-MS (System A): Rt 2.49 mins, Mass Spectrum m/z 472 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-1fe2c15411214ce3a638fb3c17203d8a |
| Source note | uspto-grants-2007_01 |