HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromophenylacetate → Ethyl {2-[({[(4-chlorophenyl)amino]carbonyl}amino)methyl]morpholin-4-yl}(phenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromophenylacetate | HCID 97780 | — |
| Reactant | N-(4-Chlorophenyl)-N'-(morpholin-2-ylmethyl)urea | HCID 23089254 | — |
| Product | Ethyl {2-[({[(4-chlorophenyl)amino]carbonyl}amino)methyl]morpholin-4-yl}(phenyl)acetate | HCID 10274401 | 232.3% |
Reaction Steps
Example 44 was prepared in an analogous manner to Example 19 using a mixture of Intermediate 9 (0.01 g) and ethyl bromo(phenyl)acetate (0.029 g) to give the title compound (0.0372 g). LC-MS (System A): Rt 3.43 mins, Mass Spectrum m/z 432 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07157457B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-575f1b3cad194be6b7f93e221a9a2610 |
| Source note | uspto-grants-2007_01 |