N-[cis-4-(Boc-amino)cyclohexyl]methanesulfonamide → HCID 86760349, compound

Participants

Reaction Steps

The compound obtained from step A was dissolved in 50% trifluoroacetic acid/dichloromethane and the mixture was stirred at room temperature for 30 minutes. The excess acid was removed under reduced pressure and the residue was triturated with ether to give a white powder, 1.51 g, 90% for two steps. MS(ES) (M+H)+=193.

Provenance & Evidence