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HRID1372002

反应详情

EQUATION

反应方程式

HRID 1372002 的结构方程式

REACTANTS

反应物

5
结构：CCOCC.FB(F)F
HCID8000

Ethane, 1,1'-oxybis-, compd. with trifluoroborane (1:1)

C4H10BF3O

结构：NN
HCID9321

Hydrazine

H4N2

结构：CCOC(=O)C(F)(F)F
HCID9794

Ethyl trifluoroacetate

C4H5F3O2

结构：C#Cc1cccc(F)c1
HCID520218

3-Fluorophenylacetylene

C8H5F

结构：[Li]CCCC
HCID178418339

未命名化合物

PRODUCTS

生成物

1
结构：Fc1cccc(-c2cc(C(F)(F)F)n[nH]2)c1
HCID178505646

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Following protocol H, 1-Ethynyl-3-fluoro-benzene was treated with n-BuLi, CF3CO2Et and BF3-OEt2 in THF. Reaction with hydrazine in benzene under similar reaction conditions yielded title compound.

WORKUP

后处理

  1. customunder similar reaction conditions