Phthalazine-5,8-dione → HCID 21072872, compound

Participants

Reaction Steps

333 mg (2.07 mmol) of phthalazin-5,8-dione (1.00 g, 6.20 mmol) and 4-methoxybenzyl azide were dissolved in 60 ml of ethyl acetate, and then refluxed overnight. The solvent was removed under reduced pressure and residue was separated and purified by using column chromatography (ethyl acetate). 415 mg of brown powder was obtained and the yield was 62%.

Provenance & Evidence