HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(2-methyl-4-oxobutan-2-yl)carbamate → HCID 86622284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(2-methyl-4-oxobutan-2-yl)carbamate | HCID 11788901 | — |
| Reactant | HCID 21072832 | HCID 21072832 | — |
| Product | HCID 86622284 | HCID 86622284 | — |
Reaction Steps
The product is obtained analogously to intermediate product 1b starting from 3-(2-amino-4-fluoro-phenyl)-pentan-3-ol and tert-butyl (1,1-dimethyl-3-oxo-propyl)-carbamate. The crude product is purified by column chromatography (silica gel, dichloromethane/MeOH 100:0→98:2). Yield: 7.70 g (99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160882B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-7db84a7244314d079394a87ccd4b3377 |
| Source note | uspto-grants-2007_01 |