HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(2-methyl-4-oxobutan-2-yl)carbamate → HCID 86600981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(2-methyl-4-oxobutan-2-yl)carbamate | HCID 11788901 | — |
| Reactant | HCID 21072831 | HCID 21072831 | — |
| Product | HCID 86600981 | HCID 86600981 | — |
Reaction Steps
The product is obtained analogously to intermediate product 1b starting from 3-(2-amino-3-methoxy-phenyl)-pentan-3-ol and tert-butyl (1,1-dimethyl-3-oxo-propyl)-carbamate. The crude product is purified by column chromatography (silica gel, cyclohexane/EtOAc 4:1). Yield: 4.60 g (47%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160882B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-69339da2b6c94b8485d797343cb97ec1 |
| Source note | uspto-grants-2007_01 |