HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,3,3,3-Pentafluoropropylamine → HCID 86596821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,3,3,3-Pentafluoropropylamine | HCID 79002 | — |
| Reactant | HCID 69040064 | HCID 69040064 | — |
| Product | HCID 86596821 | HCID 86596821 | — |
Reaction Steps
In an analogous manner to that described in Example 1 c), the condensation of (2S)-2-fluoro-2-methyl-N-[(S)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-malonamic acid and 2,2,3,3,3-pentafluoro-propylamine yielded the title compound as a white solid; MS: m/e=474 (M+H)+; optical integrity 96.4% d.e.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160875B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-fc54916d1c9b42e99e223d31dffd1ae4 |
| Source note | uspto-grants-2007_01 |