HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,4,4,4-Pentafluorobutan-1-amine → HCID 86596828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,4,4,4-Pentafluorobutan-1-amine | HCID 15754740 | — |
| Reactant | HCID 69043616 | HCID 69043616 | — |
| Product | HCID 86596828 | HCID 86596828 | — |
Reaction Steps
(S)-N-((S)-5-cyclopropylmethyl-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl)-2-fluoro-2-methyl-malonamic acid was coupled with 3,3,4,4,4-pentafluoro-butylamine in analogy to the procedure described for example 73 to yield (R)-N-((S)-5-cyclopropylmethyl-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl)-2-fluoro-2-methyl-N′-(3,3,4,4,4-pentafluoro-butyl)-malonamide as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160875B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-6bbc59969d5d4ecc89e890f44313393e |
| Source note | uspto-grants-2007_01 |