HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[N-Acetyl-N-(2-trifluoroacetylamino-ethyl)-amino]-nitrobenzene → 4-[N-acetyl-N-(2-trifluoroacetylamino-ethyl)-amino]-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[N-Acetyl-N-(2-trifluoroacetylamino-ethyl)-amino]-nitrobenzene | HCID 18005797 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-[N-acetyl-N-(2-trifluoroacetylamino-ethyl)-amino]-aniline | HCID 12047001 | — |
Reaction Steps
0.7 g (2.1 mmol) of 4-[N-acetyl-N-(2-trifluoroacetylamino-ethyl)-amino]-nitrobenzene are dissolved in 20 ml of methanol and after the addition of 100 mg of 10% palladium on activated charcoal hydrogenated with hydrogen for 3 hours. Then the catalyst is filtered off and evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160901B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-c364b1ab2c374c409ed4be9aaca699e3 |
| Source note | uspto-grants-2007_01 |