HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18005810, compound → HCID 18005730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18005810 | HCID 18005810 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18005730 | HCID 18005730 | — |
Reaction Steps
450 mg (1.26 mmol) of 4-[N-(2-benzyloxycarbonylamino-ethyl)-N-acetyl-amino)-nitrobenzene (prepared analogously to Example I) are dissolved in 20 ml of methanol and after the addition of 100 mg of Lindlar catalyst hydrogenated for 2 hours with hydrogen. The catalyst is filtered off, the solution is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160901B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-ba7e5cb951964af38dd0760d19363fc8 |
| Source note | uspto-grants-2007_01 |