HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → N~1~-(3-Hydroxypropyl)ethanediamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | N-(2-hydroxyethyl)oxalamide | HCID 5249043 | — |
| Product | N~1~-(3-Hydroxypropyl)ethanediamide | HCID 14935787 | 75% |
Reaction Steps
Prepared as in Intermediate 3, using 3-aminopropanol to give the title compound as a white powder (1.15 g, 75%); NMR [(CD3)2SO] 1.6 (2H, m), 3.18 (2H, m), 3.42 (2H, m), 4.47 (1H, t), 7.73 (1H, br s), 8.0 (1H, br s), and 8.63 (1H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160907B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-95bbbdf359e249be9cc1fc636739ee1a |
| Source note | uspto-grants-2007_01 |