HCID 21073115, compound → HCID 21073113, compound

Participants

Reaction Steps

10% carbon-palladium (0.2 g) was added to an ethanol (20 ml) solution of tert-butyl[4-(2-nitrophenoxy)benzyl]carbamate (1.43 g, 4.15 mmols). The resulting mixture was hydrogenated at room temperature under atmospheric pressure. The catalyst was removed through filtration, and the filtrate was concentrated under reduced pressure. An oil of tert-butyl[4-(2-aminophenoxy)benzyl]carbamate (1.13 g, 86.9%) was obtained.

Provenance & Evidence