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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1373340Generated: October 30, 2026

Toluene → HCID 21361290, compound

https://huagongshe.com/reaction/1373340

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTolueneHCID 1140—
ReactantTriethylamineHCID 8471—
ReactantHCID 22341826HCID 22341826—
ProductHCID 21361290HCID 2136129091%

Reaction Steps

In analogy to example 1 were reacted 6.1 g (2 mmol) of 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-ol (prepared as described in GB 2335190, compound 110) with 4.38 g (2 mmol) of lauroyl chloride chloride and 2.02 g (2 mmol) of triethylamine in toluene to give 8.9 g (91%) dodecanoic acid 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-yl ester as yellowish liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07160966B2
Source datasetuspto-grants-2007_01
ORD IDord-b179ba9e3c0e45cbb2aace519d54a02c
Source noteuspto-grants-2007_01