HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 21361290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 22341826 | HCID 22341826 | — |
| Product | HCID 21361290 | HCID 21361290 | 91% |
Reaction Steps
In analogy to example 1 were reacted 6.1 g (2 mmol) of 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-ol (prepared as described in GB 2335190, compound 110) with 4.38 g (2 mmol) of lauroyl chloride chloride and 2.02 g (2 mmol) of triethylamine in toluene to give 8.9 g (91%) dodecanoic acid 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-yl ester as yellowish liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07160966B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-b179ba9e3c0e45cbb2aace519d54a02c |
| Source note | uspto-grants-2007_01 |