Sodium Hydroxide → Cyclopentanone, 2-(1-hydroxypentyl)-
反応式
[OH-:1].[Na+].[CH:3](=[C:8]1[CH2:12][CH2:11][CH2:10][C:9]1=[O:13])[CH2:4][CH2:5][CH2:6][CH3:7]>>[OH:1][CH:3]([CH:8]1[CH2:12][CH2:11][CH2:10][C:9]1=[O:13])[CH2:4][CH2:5][CH2:6][CH3:7]参加物
3
実験手順
Additional 15.8 g (0.19 mol) 48% NaOH was added thereto, and the mixture was stirred at the same temperature for 2 hours. After the reaction was finished, the mixture was neutralized and analyzed in the same manner as in Example 1. The result indicated that the reaction mixture contained 521 g (3.06 mol) 2-(1-hydroxy-n-pentyl)cyclopentanone (yield 83.8%) and 18.2 g (0.119 mol) 2-pentylidene cyclopentanone.
出典と根拠
- ORDレコード
- ord-915382beefce43c8b12b111ce79a8e57
- 出典データセット
- uspto-grants-2007_01
- 特許番号
- US07161041B2
反応ノート
読み込み中…