Acryloyl chloride → 1-ADAMANTYL ACRYLATE
Reaction equation
[C:1]12([OH:11])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:12](Cl)(=[O:15])[CH:13]=[CH2:14]>>[C:12]([O:11][C:1]12[CH2:8][CH:7]3[CH2:6][CH:5]([CH2:4][CH:3]([CH2:9]3)[CH2:2]1)[CH2:10]2)(=[O:15])[CH:13]=[CH2:14]Participants
3
Procedure
1-Adamantanol and acrylic acid chloride were subjected to desalting reaction by using a basic catalyst to obtain adamantyl acrylate (Compound (III-h)).
Workup
- customreaction
Sources & evidence
- ORD record
- ord-2860dc8f79df4a72a57d34195026fded
- Source dataset
- uspto-grants-2007_01
- Patent number
- US07163781B2
Reaction notes
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