HRID1373721

反应详情

EQUATION

反应方程式

HRID 1373721 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

4.2 g of the nitro compound from example k in 120 ml MeOH were hydrogenated at atmospheric pressure with 10% Pd—C at room temperature for 3 hrs. The mixture was filtered and the filtrate evaporated to yield 3.13 g of the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. customthe filtrate evaporated