HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(hydroxymethyl)benzoate → HCID 69318823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(hydroxymethyl)benzoate | HCID 81325 | — |
| Reactant | HCID 69317190 | HCID 69317190 | — |
| Product | HCID 69318823 | HCID 69318823 | — |
Reaction Steps
The title compound was prepared employing the procedure in Example 2 using (R)-2-(4-chloro-benzenesulfonylamino)-2-(4-fluoro-phenyl)-acetamide and methyl-4-hydroxymethylbenzoate to afford the desired product. Diagnostic 13CNMR (100 MHz, CDCl3) 49.9, 52.3, 63.4, 116.0, 116.2, 127.9, 129.1, 129.5, 129.6, 132.0, 132.1, 139.8, 142.3. MS 491.2 m/z (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07163942B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-ff89882c436043e5b45c8f27d7806f44 |
| Source note | uspto-grants-2007_01 |