HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 16638811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57488769 | HCID 57488769 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 16638811 | HCID 16638811 | — |
Reaction Steps
2-Bromo-5-(1-methylethoxy)-4-methoxybenzene acetaldehyde (2.60 g, 9.05 mmol) is added at 15° C. within 30 minutes to a suspension of sodium borohydride (0.341 g, 9.05 mmol) in absolute ethanol (40 ml), and it is stirred for two hours at this temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166588B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-e0d883e92b104a18b82704715825d718 |
| Source note | uspto-grants-2007_01 |