HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 69413866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | N-Desmethylgalanthamine | HCID 9838394 | — |
| Reactant | HCID 21076643 | HCID 21076643 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 69413866 | HCID 69413866 | — |
Reaction Steps
Norgalanthamine (1.13 g, 1.64 mmol), 5-(6-iodo-1-oxohexyl)-5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-2(1H)-one (1.50 g, 3.75 mmol) and N-ethyldiisopropylamine (1.46 g, 11.3 mmol) are stirred in absolute chloroform (20 ml) for 54 hours at boiling temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166588B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-5d0f4817c29a4cabbe103870860f63ac |
| Source note | uspto-grants-2007_01 |